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ASTM C1347-08(2023)

Current Reaffirmation

Standard Practice for Preparation and Dissolution of Uranium Materials for Analysis

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1.1 This practice covers dissolution treatments for uranium materials that are applicable to the test methods used for characterizing these materials for uranium elemental, isotopic, and impurities determinations. Dissolution treatments for the major uranium materials assayed for uranium or analyzed for other components are listed.

1.2 The treatments, in order of presentation, are as follows:

Procedure Title

Section

Dissolution of Uranium Metal and Oxide with Nitric Acid

8.1

Dissolution of Uranium Oxides with Nitric Acid and Residue
  Treatment

8.2

Dissolution of Uranium-Aluminum Alloys in Hydrochloric Acid
 with Residue Treatment

8.3

Dissolution of Uranium Scrap and Ash by Leaching with Nitric
 Acid and Treatment of Residue by Carbonate Fusion

8.4

Dissolution of Refractory Uranium-Containing Material by
 Carbonate Fusion

8.5

Dissolution of Uranium—Aluminum Alloys
Uranium Scrap and Ash, and Refractory
Uranium-Containing Materials by
Microwave Treatment

8.6

1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific hazards statements are given in Section 7.

1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.


4.1 The materials covered that must meet ASTM specifications are uranium metal and uranium oxide.

4.2 Uranium materials are used as nuclear reactor fuel. For this use, these materials must meet certain criteria for uranium content, uranium-235 enrichment, and impurity content, as described in Specifications C753 and C776. The material is assayed for uranium to determine whether the content is as specified.

4.3 Uranium alloys, refractory uranium materials, and uranium containing scrap and ash are unique uranium materials for which the user must determine the applicability of this practice. In general, these unique uranium materials are dissolved with various acid mixtures or by fusion with various fluxes.

SDO ASTM: ASTM International
Document Number C1347
Publication Date Jan. 1, 2023
Language en - English
Page Count 9
Revision Level 08(2023)
Supercedes
Committee C26.05
Publish Date Document Id Type View
June 1, 2014 C1347-08R14E01 Revision
Dec. 1, 2008 C1347-08 Revision
Aug. 10, 2002 C1347-02 Revision
Jan. 1, 2023 C1347-08R23 Reaffirmation